A New Coprecipitation Methodology with Lutetium Hydroxide for Preconcentration of Heavy Metal Ions in Herbal Plant Samples


SOYLAK M. , Murat I.

JOURNAL OF AOAC INTERNATIONAL, cilt.97, ss.1189-1194, 2014 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 97 Konu: 4
  • Basım Tarihi: 2014
  • Doi Numarası: 10.5740/jaoacint.12-331
  • Dergi Adı: JOURNAL OF AOAC INTERNATIONAL
  • Sayfa Sayıları: ss.1189-1194

Özet

A new coprecipitation methodology that used lutetium hydroxide as a precipitant for Cu(II), Pb(II), Mn(II), Co(II), Cd(II), Fe(III), and Ni(II) ions in herbal plant and water samples for analysis by atomic absorption spectrometry has been investigated. The parameters such as pH, amount of lutetium, and volume of aqueous sample were optimized for the recovery of these seven metals. The effects of concomitant ions on the separation-preconcentration of analytes were also checked. The validation of the procedure was checked with addition recovery tests and analysis of Standard Reference Material 1570a-Trace Elements in Spinach Leaves and TMDA-70 fortified lake water Certified Reference Material. The LODs for analyte ions were in the range of 1.7-7.2 mu g/L. The application of the present procedure was successfully performed for the analysis of analyte contents of herbal plant samples from Turkey.