DETERMINATIONS OF SOME TRACE-METALS IN DIALYSIS SOLUTIONS BY ATOMIC-ABSORPTION SPECTROMETRY AFTER PRECONCENTRATION


SOYLAK M., elçi l., doğan m.

ANALYTICAL LETTERS, vol.26, no.9, pp.1997-2007, 1993 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 26 Issue: 9
  • Publication Date: 1993
  • Doi Number: 10.1080/00032719308017446
  • Journal Name: ANALYTICAL LETTERS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.1997-2007
  • Keywords: DIALYSIS SOLUTION, CU, PB, FE, CD, CO, NI, AMBERLITE XAD-4, AAS, HEMODIALYSIS, ELEMENTS
  • Erciyes University Affiliated: Yes

Abstract

A method is presented for the determination of copper, lead, iron, cadmium, cobalt and nickel in dialysis solution at mu/l level by atomic absorption spectrometry after preconcentration. The preconcentration is based on chelate formation of the investigated metals with ammonium pyrrolydine dithiocarbamate and on retention of the chelates on Amberlite XAD-4 in a short column. The relative standard deviations for the determinations were found to be lower than 0.08.