Crystal structure of 1,4-dihydroxy-3,4-dibromo-1,2,3,4-tetrahydro-naphthalene


Ozturk S., Buyukkidan B., Erenler R., Akkurt M. , Cakmak O., Fun H.

CRYSTAL RESEARCH AND TECHNOLOGY, cilt.39, ss.815-820, 2004 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 39 Konu: 9
  • Basım Tarihi: 2004
  • Doi Numarası: 10.1002/crat.200310259
  • Dergi Adı: CRYSTAL RESEARCH AND TECHNOLOGY
  • Sayfa Sayıları: ss.815-820

Özet

The title compound (C10H10O2Br2) crystallizes in the orthorhombic space group P2(1)2(1)2(1) with a 5.0319(2)Angstrom, b = 13.5282(5)Angstrom, c = 15.6289(6)Angstrom, V = 1063.90(1)Angstrom(3), Z = 4, D = 2.01 g/cm(3) at T = 293(2)K. The structure was solved by direct methods and refined by full-matrix least-squares procedures to final R = 0.078 and wR = 0.140 using 1212 observed reflections with [I greater than or equal to 2sigma(I)]. The title compound as a whole is not planar. The crystal structure is stabilized by hydrogen contacts and weak van der Waals interactions.