Crystal structure of (5Z)-5-(5-bromo-2-hydroxybenzylidene)-1,3-thiazolidine-2,4-dioney

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Mague J. T., Mohamed S. K., AKKURT M., Younes S. H. H., Albayati M. R.

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, vol.71, 2015 (ESCI)

• Publication Type: Article / Article
• Volume: 71
• Publication Date: 2015
• Doi Number: 10.1107/s2056989015020654
• Journal Name: ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS
• Journal Indexes: Emerging Sources Citation Index (ESCI), Scopus
• Erciyes University Affiliated: Yes

Abstract

In the title compound, C10H6BrNO3S, the dihedral angle between the thiazolidine ring (r.m.s. deviation = 0.014 angstrom) and the benzene ring is 5.78 (14)degrees. The S atom of the heterocyclic ring is syn to the OH group attached to the benzene ring. In the crystal, inversion dimers linked by pairs of N-H center dot center dot center dot O hydrogen bonds generate R-2(2)(8) loops. The dimers are linked into [001] ribbons by pairwise O-H center dot center dot center dot O hydrogen bonds with R-2(2)(18) motifs. There are no short contacts involving the Br atom.