Multiwalled carbon nanotube impregnated with tartrazine: Solid phase extractant for Cd(II) and Pb(II)

SOYLAK M., Topalak Z.

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, vol.20, no.2, pp.581-585, 2014 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 20 Issue: 2
  • Publication Date: 2014
  • Doi Number: 10.1016/j.jiec.2013.05.017
  • Journal Name: JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.581-585
  • Keywords: Multiwalled carbon nanotube, Tartrazine, Impregnation, Flame atomic absorption spectrometry, ATOMIC-ABSORPTION-SPECTROMETRY, HEAVY-METAL IONS, NATURAL-WATER SAMPLES, TRACE-ELEMENT LEVELS, RARE-EARTH-ELEMENTS, AMBERLITE XAD-16, ACTIVATED CARBON, COLUMN PRECONCENTRATION, IRON DETERMINATION, CLOUD POINT
  • Erciyes University Affiliated: Yes

Abstract

A solid phase extraction procedure has been presented by using multiwalled carbon nanotube impregnated with tartrazine for cadmium (Cd(II)) and lead (Pb(II)) ions. The influences of pH, flow rate, eluent and sample volume were investigated. No interference effects were observed from the alkaline, alkaline earth and some transition metals. The detection limits (LOD) were 0.8 and 6.6 mu g L-1 for Cd(II) and Pb(II), respectively. The preconcentration factor was 40. The validation of the procedure was controlled by the analysis of certified references materials. The procedure was applied to the determination of cadmium and lead in natural water and food samples. (C) 2013 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.