Crystal structure of 3-benzyl-1-[(1,2,3,4-tetrahydronaphthalen-1-ylidene)amino]-thiourea

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Mohamed S. K., Mague J. T., AKKURT M., Hassan A. A., Abdel-Aziz A. T., Albayati M. R.

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, vol.71, 2015 (ESCI)

• Publication Type: Article / Article
• Volume: 71
• Publication Date: 2015
• Doi Number: 10.1107/s2056989015021064
• Journal Name: ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS
• Journal Indexes: Emerging Sources Citation Index (ESCI), Scopus
• Erciyes University Affiliated: Yes

Abstract

In the title compound, C18H19N3S, the dihedral angle between the planes of the benzene rings is 58.63 (8)degrees. The six-membered ring bonded to the thiosemicarbazide group (r.m.s. deviation = 0.038 angstrom) adopts a sofa conformation, with one of the methylene-group C atoms as the flap. A short intramolecular N-H center dot center dot center dot N contact is observed. In the crystal, molecules are linked by weak N-H center dot center dot center dot S interactions to generate C(4) chains propagating in the [010] direction, with adjacent molecules related by glide symmetry.