MnO2 nanowires as an effective and nano sorbent for dispersive micro solid phase extraction of copper from food and water samples

SOYLAK M., Mohammed A. M. A., UZCAN F.

Journal of Food Composition and Analysis, cilt.144, 2025 (SCI-Expanded, Scopus) identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 144
  • Basım Tarihi: 2025
  • Doi Numarası: 10.1016/j.jfca.2025.107733
  • Dergi Adı: Journal of Food Composition and Analysis
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, PASCAL, Analytical Abstracts, BIOSIS, Biotechnology Research Abstracts, CAB Abstracts, Food Science & Technology Abstracts, Veterinary Science Database
  • Anahtar Kelimeler: Environmental monitoring, Food safety, Green chemistry, Heavy metals, Trace analysis
  • Erciyes Üniversitesi Adresli: Evet

Özet

Manganese oxide nanowires were synthesized and used as a sorbent for the dispersive micro-solid-phase extraction method to extract copper from water and food samples. X-ray diffraction, field emission scanning electron microscopy, Fourier transform infrared spectroscopy, and scanning transmission electron microscopy were used to analyze the sorbent. The parameters impacting extraction efficiency were also investigated and optimized in the study. A pH of 7.0, 1 mg of adsorbent, 2.5 minutes for both desorption and adsorption, and 3 mol L−1 HNO3 as the desorption solvent were determined to be the optimum working conditions. The relative recoveries ranged from 91 % to 105 %, and the detection limit was 2.9 ng mL−1. This technique is emphasized for being quick, accurate, and eco-friendly, making it a practical option for detecting the amount of copper in food and water samples.