Membrane Filtration of Nickel(II) on Cellulose Acetate Filters for Its Preconcentration, Separation, and Flame Atomic Absorption Spectrometric Determination


SOYLAK M. , ünsal Y. E. , aydın A., kızıl N.

CLEAN-SOIL AIR WATER, cilt.38, ss.91-95, 2010 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 38 Konu: 1
  • Basım Tarihi: 2010
  • Doi Numarası: 10.1002/clen.200900189
  • Dergi Adı: CLEAN-SOIL AIR WATER
  • Sayfa Sayıları: ss.91-95

Özet

An enrichment method for trace amounts of Ni(II), as 8-hydroxyquinoline chelates, has been established on a cellulose acetate membrane filter. Ni(II)-8-hydroxyquinoline chelates adsorbed on a membrane filter were eluted using 5 mL of 1 M HNO(3). The eluent nickel concentration was determined by a flame atomic absorption spectrometer. The influence of some analytical parameters, including pH, amount of reagent, sample volume, etc., on recovery was investigated. The interference of co-existent ions was studied. The nickel detection limit was 4.87 mu g/L. The method was applied to real samples for the determination of nickel(II) ions.