Tetracyanoethylene as a mediator and building block in synthesis of 5-substituted amino-1,3,4-thiadiazolyl-1H-pyrazole derivatives

Hassan, Alaa; Mohamed, Shaaban; Abdel-Latif, Fathy; Mostafa, Sara; Mague, Joel; AKKURT, MEHMET; Abdel-Aziz, Mohamed

doi:10.1016/j.tetlet.2015.12.023

Tetracyanoethylene as a mediator and building block in synthesis of 5-substituted amino-1,3,4-thiadiazolyl-1H-pyrazole derivatives

Hassan A. A., Mohamed S. K., Abdel-Latif F. F., Mostafa S. M., Mague J. T., AKKURT M., ...Daha Fazla

TETRAHEDRON LETTERS, cilt.57, sa.3, ss.345-347, 2016 (SCI-Expanded, Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 57 Sayı: 3
Basım Tarihi: 2016
Doi Numarası: 10.1016/j.tetlet.2015.12.023
Dergi Adı: TETRAHEDRON LETTERS
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.345-347
Erciyes Üniversitesi Adresli: Evet

Özet

The conversion of thiocarbonohydrazides to 5-substituted amino-1,3,4-thiadiazolyl-1H-pyrazoles in one-step was achieved via the reaction with tetracyanoethylene (TCNE). In this conversion, TCNE is used as a mediator and/or a building block. The product was conclusively confirmed by spectroscopic data and single crystal X-ray structural analysis. (C) 2015 Elsevier Ltd. All rights reserved.