Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p '-dimethoxybenzoyl acetic acid hydrazide

ULKU, D; ARICI, C; ERCAN, F; SACMACI, Mustafa; Saripinar, EMİN; AKCAMUR, Yunus

doi:10.1524/zkri.218.5.377.20737

Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p '-dimethoxybenzoyl acetic acid hydrazide

ULKU D., ARICI C., ERCAN F., SACMACI M., Saripinar E., AKCAMUR Y.

ZEITSCHRIFT FUR KRISTALLOGRAPHIE, cilt.218, sa.5, ss.377-380, 2003 (SCI-Expanded, Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 218 Sayı: 5
Basım Tarihi: 2003
Doi Numarası: 10.1524/zkri.218.5.377.20737
Dergi Adı: ZEITSCHRIFT FUR KRISTALLOGRAPHIE
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.377-380
Erciyes Üniversitesi Adresli: Hayır

Özet

The structure of the organic derivative of N-p-methylbenzyliden-N-phenyl-p,p'-dimethoxybenzoyl acetic acid hydrazide, [C32H28N2O5], has been determined by X-ray diffraction. The structure derived from the NMR spectroscopy, the IR spectra and elemental analysis is consistent with that of the X-ray diffraction. The compound crystalizes in the monoclinic system with space group P21/c, a = 16.234(1), b = 9.399(2), c = 19.389(1), beta = 110.924(3)degrees, V = 2763.3(5) Angstrom(3) and Z = 4. In the crystal, there is one weak C-H...O type intermolecular hydrogen bond interaction.