Column separation and enrichment of trace amounts of Cu, Ni and Fe on XAD-16 resin in industrial fertilizers after complexation with 4-(2-Thiazolylazo) resorcinol
JOURNAL OF TRACE AND MICROPROBE TECHNIQUES, cilt.15, sa.2, ss.197-204, 1997 (SCI-Expanded, Scopus)
- Yayın Türü: Makale / Tam Makale
- Cilt numarası: 15 Sayı: 2
- Basım Tarihi: 1997
- Dergi Adı: JOURNAL OF TRACE AND MICROPROBE TECHNIQUES
- Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
- Sayfa Sayıları: ss.197-204
- Anahtar Kelimeler: preconcentration, separation, amberlite XAD-16, fertilizers, Cu, Ni, Fe, 4-(2-Thiazolylazo) resorcinol, AAS
- Erciyes Üniversitesi Adresli: Evet
Özet
A simple and rapid method has been established for determination of trace amounts of copper, iron and nickel after separation and preconcentration by sorbing the metal/4-(2-Thiazolylazo) resorcinol (TAR) complexes on amberlite XAD-16 resin. The method was applied to the determination of these ions in industrial fertilizers with good results such as recoveries more than 95%, relative standard deviations 3 to 5% (N = 10) and detection limits under 40 ng/l.