1,3-Bis(2-chlorobenzoyl)-3,4,5,6-tetrahydropyrimidine-2(1H)-thione


Yildirim S. O. , Akkurt M. , Genc M., Sekerci M., Fun H. -.

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, cilt.62, 2006 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 62
  • Basım Tarihi: 2006
  • Doi Numarası: 10.1107/s1600536806030236
  • Dergi Adı: ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE

Özet

The title compound, C(18)H(14)Cl(2)N(2)O(2)S, was synthesized by the reaction of 1,4,5,6-tetrahydropyrimidine-2-thiol and 2-chlorobenzoyl chloride. The dihedral angle between the two chlorobenzene rings is 76.2 (1)degrees. The ring carbon ( and attached H atoms) opposite the C S group are disordered over two sites. In the crystal structure, there is one intermolecular C - H(...)O and one intramolecular C - H(...)N hydrogen bond.