1,3-Bis(2-chlorobenzoyl)-3,4,5,6-tetrahydropyrimidine-2(1H)-thione


Yildirim S. , Akkurt M. , Genc M., Sekerci M., Fun H. -.

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, vol.62, 2006 (Journal Indexed in SCI) identifier identifier

  • Publication Type: Article / Article
  • Volume: 62
  • Publication Date: 2006
  • Doi Number: 10.1107/s1600536806030236
  • Title of Journal : ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS

Abstract

The title compound, C18H14Cl2N2O2S, was synthesized by the reaction of 1,4,5,6-tetrahydropyrimidine-2-thiol and 2-chlorobenzoyl chloride. The dihedral angle between the two chlorobenzene rings is 76.2 (1)degrees. The ring carbon ( and attached H atoms) opposite the C S group are disordered over two sites. In the crystal structure, there is one intermolecular C - (HO)-O-... and one intramolecular C - (HN)-N-... hydrogen bond.