STRUCTURE OF 1-AMINO-5-BENZOYL-4-PHENYL-1H-PYRIMIDINE-2-THIONE


AKKURT M. , GULDESTE A. , SOYLU H. , ALTURAL B. , SARIPINAR E.

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, cilt.48, ss.315-317, 1992 (SCI İndekslerine Giren Dergi) identifier

  • Cilt numarası: 48
  • Basım Tarihi: 1992
  • Doi Numarası: 10.1107/s0108270191008910
  • Dergi Adı: ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
  • Sayfa Sayıları: ss.315-317

Özet

C17H13N3OS, M(r) = 307.38, monoclinic, P2(1)/n, a = 9.712 (3), b = 15.072 (3), c = 10.713 (3) angstrom, beta = 107.65 (3)-degrees, V = 1494.34 angstrom 3, Z = 4, D(m) = 1.372, D(x) = 1.366 g cm-3, Mo K-alpha, lambda = 0.71069 angstrom, mu = 2.11 cm-1, F(000) = 640, T = 295 K, final R(F) = 0.0417 for 2608 unique reflections. The pyrimidine ring is almost planar, the angle between the planes formed by the ring atoms N1-C6-C5 and C2-N3-C4 being 0.74-degrees.