Spectrophotometric determination of iodine by iodine starch method in urine samples after alkaline ashing

DİVRİKLİ Ü., Soylak M., doğan m.

CHEMIA ANALITYCZNA, cilt.45, sa.2, ss.257-264, 2000 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 45 Sayı: 2
  • Basım Tarihi: 2000
  • Dergi Adı: CHEMIA ANALITYCZNA
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.257-264
  • Anahtar Kelimeler: iodine, drinking water, urine, alkaline ashing, iodine-starch method, spectrophotometry, MILK
  • Erciyes Üniversitesi Adresli: Evet

Özet

A spectrophotometric method is proposed for the determination of iodine in urine samples. Destruction of the organic matter of urine by alkaline ashing with KOH is carried out prior to determination of iodine by the iodine-starch method. The influence of components of urine, as interferents, was discussed. The iodine contents of the urine samples collected from adults from Kayseri (Turkey) were determined by using the proposed method. The method was also applied for the determination of iodine in drinking water samples. The relative standard deviations of the iodine determinations were less than 10%. The detection limit of the proposed method was 2.3 mu g l(-1).