1,3-Bis(2-chlorobenzoyl)-3,4,5,6-tetrahydropyrimidine-2(1H)-thione

Yildirim, SEMA; Akkurt, MEHMET; Genc, Murat; Sekerci, Memet; Fun, H.

doi:10.1107/s1600536806030236

1,3-Bis(2-chlorobenzoyl)-3,4,5,6-tetrahydropyrimidine-2(1H)-thione

Atıf İçin Kopyala

Yildirim S., Akkurt M., Genc M., Sekerci M., Fun H. -.

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, cilt.62, 2006 (SCI-Expanded)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 62
Basım Tarihi: 2006
Doi Numarası: 10.1107/s1600536806030236
Dergi Adı: ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Emerging Sources Citation Index (ESCI), Scopus
Erciyes Üniversitesi Adresli: Evet

Özet

The title compound, C18H14Cl2N2O2S, was synthesized by the reaction of 1,4,5,6-tetrahydropyrimidine-2-thiol and 2-chlorobenzoyl chloride. The dihedral angle between the two chlorobenzene rings is 76.2 (1)degrees. The ring carbon ( and attached H atoms) opposite the C S group are disordered over two sites. In the crystal structure, there is one intermolecular C - (HO)-O-... and one intramolecular C - (HN)-N-... hydrogen bond.